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Dairy Titration

TitraLab 845
Routine Potentiometric Titration Workstation (Bi burette)

With the new multi-technique TitraLab 845 bi-burette titration workstation you can benefit from superior quality results at the touch of a button. Ideal for routine applications, its use is simpler than ever before. The TitraLab 845 represents today the best value for money on the market for routine potentiometric titrations.

TitraLab 845

Total acidity in milk
Salt content in butter
Acidity in cheese
Chloride in milk, butter, other dairy products
 Routine measurement of CIP Acid and Base strength

Acidity of Milk
The acidity of milk is determined by end point titration using 0.1 eq/l NaOH. The end point value is generally fixed at pH 8.7 and the result is expressed in dg/l of lactic acid. This result is also called DORNIC acidity.

Results for 10 determinations
Mean (as grams/100ml of lactic acid): 0.1517
Standard deviation:0.106
Relative standard deviation: 0.7%

Acidity of Milk
Click to view application note

Salt in Butter
The silver nitrate reacts with the chloride ion according to (Ag+, NO3-) + Cl- → AgCl (precipitate) + NO3- Then 1 mole of AgNO3 corresponds to 1 mole of chloride. The titrant concentration is generally 0.1M. The results are expressed as a % of salt (NaCl with a molecular weight of 58.453 g/mol).

Results for three determinations on salted butter, generally expressed as a % of sodium chloride ion (MW = 58.453 g/mol)
Mean: 1.995%
Standard deviation: 0.0018%
Rel. standard deviation: 0.09%
(Butter with a salt content of 2%) 

Results for three determinations on butter (with a 10 ml burette), generally expressed as a % of sodium chloride ion (MW = 58.453 g/mol)
Mean: 0.036%
Standard deviation: 0.0003%
Rel. standard deviation: 0.8%

Salt in Butter
Click to view application note

Acidity of Cheese
The acidity of cheese is determined by end point titration using 0.1 eq/l NaOH. The end point value is generally fixed at pH 8.4 and the result is expressed in % of lactic acid, which has a MW of 90.08 g/mol.

Results for 5 determinations, expressed as % of lactic acid (CH3-CHOH-COOH with a MW of 90.08 g/mol)
Mean: 0.97%
Standard deviation: 0.01%
Rel. standard deviation: 1%

Acidity of Cheese
Click to view application note

TitraLab 845 Technical Specifications

Methods
End point titration: 1 to 2 preset end points.
Inflection point titration: Auto determination of 1 to 4 inflection points, programmable IP acceptation windows.
IP detection using 1st & 2nd derivative curve.
Titration stops at: pH, mV, ml, IP number.
Titrant addition techniques: incremental dynamic, incremental monotonic and continuous dynamic.
Titrant calibration.
pH electrode calibration: up to 5 points using IUPAC standards or 4-7-10 Series buffers with error recognition.
Direct pH/mV measurements: with recording on stable reading.
Back titration with manual (TIM840) or automatic (TIM845) reagent addition.
Sequencing of up to 3 consecutive methods within a sample changer series.
Coupling of 2 methods in one beaker.
 
Measuring Range
-9 to 23 pH
±2000 mV
-10°C to +100°C
 
Resolution
0.001 pH
0.1mV
0.1°C

TitraLab 845 Full Specification

For more information on this product please contact the product manager, Jamie Duncan on 01342 820820 or e-mail enquiries@qclscientific.com.

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